Process Engineering Design For Manufacture Of Guanidine Nitrate
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Process Engineering Design For Manufacture Of Guanidine Nitrate
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Author : N. W. Steele
language : en
Publisher:
Release Date : 1973
Process Engineering Design For Manufacture Of Guanidine Nitrate written by N. W. Steele and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 1973 with categories.
The report completes the technical, operating and economic studies for a 3-year pilot plant demonstration of the urea/ammonium nitrate (U/AN) route to guanidine nitrate (GN) as an intermediate for manufacture of nitroguanidine (NQ). It summarizes the 1973 effort, including plant modifications, production of 10 tons of specification GN, economic comparison of the U/AN and British Aqueous Fusion (BAF) processes for GN, and layaway of the GN pilot plant. An economic catalyst (Houdry CP-532 silica bead) lifetime was shown in the reactors which are basically production prototypes in design and size. The concept of the U/AN process for manufacturing GN via a melt reactor plus a single aqueous crystallization step was demonstrated.
Process Engineering Design For Manufacture Of Guanidine Nitrate
READ & DOWNLOAD eBooks
Author : N. W. Steele
language : en
Publisher:
Release Date : 1973
Process Engineering Design For Manufacture Of Guanidine Nitrate written by N. W. Steele and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 1973 with categories.
The object of this program was to develop design data and produce 40, 500 lb of guanidine nitrate (GN) via the catalytic reaction of ammonium nitrate (AN) and urea. Laboratory and pilot plant experiments confirmed the soundness of the process as described in the literature. Mathematical models and computer programs developed on the basis of laboratory kinetic and process variable data proved to be fully capable in predicting the behavior of packed bed tubular reactors. A semi-continuous pilot plant (nomial capacity of 50 lb GN/hr) was constructed on the basis of laboratory data. About one ton of 96+% purity GN was produced using a single aqueous crystallization step for product recovery. Total production was not met because of catalyst poisoning, which was traced to phosphates and perhaps borates in commercial grade AN. Sensitivity and hazards analyses show that no in-process material is capable of self-propagation. Preliminary economic studies indicate cost advantages over the British aqueous fusion process. Continuation of pilot plant operations to extend catalyst mileage data, particularly with recycle, and more detailed cost analysis are recommended.
Process Engineering Design For Manufacture Of Guanidine Nitrate Volume Ii Appendices
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Author : N. W. Steele
language : en
Publisher:
Release Date : 1973
Process Engineering Design For Manufacture Of Guanidine Nitrate Volume Ii Appendices written by N. W. Steele and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 1973 with categories.
The document contains appendices for a report on development of design data and a pilot plant for production of guanidine nitrate. It includes data and data processing programs relative to various process specifications, pilot plant operation, and catalyst poisoning research, safety engineering reports, and a literature search on guanidine nitrate production from urea.
Government Reports Announcements
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Author :
language : en
Publisher:
Release Date : 1974
Government Reports Announcements written by and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 1974 with Science categories.
Government Reports Announcements Index
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Author :
language : en
Publisher:
Release Date : 1979
Government Reports Announcements Index written by and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 1979 with Science categories.
A Directory Of Computer Software Applications
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Author :
language : en
Publisher:
Release Date : 1978
A Directory Of Computer Software Applications written by and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 1978 with Chemistry categories.
A Directory Of Computer Software Applications
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Author : United States. National Technical Information Service
language : en
Publisher:
Release Date : 1978
A Directory Of Computer Software Applications written by United States. National Technical Information Service and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 1978 with Chemistry categories.